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• W2330585555 abstract "The CuI complex obtained in situ from CuI and tris((4-methoxy-3,5-dimethylpyridin-2-yl)methyl)amine (TPMA*) is currently the most reducing and the most active catalyst for atom transfer radical polymerizations (ATRP). The complex has a high affinity for alkyl halides (ATRP pathway) but also has sufficient affinity toward organic radicals to potentially participate in organometallic-mediated radical polymerization (OMRP). Thus, the radical polymerization of n-butyl acrylate initiated by AIBN (azobisisobutyronitrile) was significantly retarded, and the molecular weights decreased in the presence of the CuI/TPMA* complex. These results suggest the presence of a Cu-mediated termination processes, even after the amount of radicals generated from AIBN exceeded the initial amount of CuI/TPMA*. Nevertheless, in the presence of alkyl bromides, which act as ATRP initiators for acrylates, control was gained through metal-mediated halogen atom transfer, i.e., ATRP, not OMRP." @default.
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• W2330585555 date "2012-10-31" @default.
• W2330585555 modified "2023-09-30" @default.
• W2330585555 title "Formation and Possible Reactions of Organometallic Intermediates with Active Copper(I) Catalysts in ATRP" @default.
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• W2330585555 doi "https://doi.org/10.1021/om3006883" @default.
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