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• W2330831406 endingPage "7415" @default.
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• W2330831406 abstract "The reaction of 5,10,15-tris(4-tert-butylphenyl)corrole with 2,3-bis(bromomethyl)-5,6-dicyanopyrazine provides a new example of corrole ring expansion to a hemiporphycene derivative. The ring expansion is regioselective, with insertion of the pyrazine derivative at the 5-position of the corrole ring, affording the corresponding 5-hemiporphycene. Different macrocyclic products accompany formation of the 5-hemiporphycene, depending on the reaction experimental conditions. Br-substitued 5-hemiporphycenes and the 2-Br substituted corrole were obtained in 1,2,4-trichlorobenzene, while in refluxing toluene traces of an inner core substituted corrole were observed together with a significant amount of the unreacted corrole. These results provide an important indication of the reaction pathway. The coordination behavior of the 5-hemiporphycene, together with detailed electrochemical characterization of the free-base and some metal complexes, provides evidence for the reactivity of the peripheral pyrazino group." @default.
• W2330831406 created "2016-06-24" @default.
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• W2330831406 date "2014-06-30" @default.
• W2330831406 modified "2023-10-16" @default.
• W2330831406 title "New Example of Hemiporphycene Formation from the Corrole Ring Expansion" @default.
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• W2330831406 doi "https://doi.org/10.1021/ic500757a" @default.
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