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- W2331261126 abstract "Abstract Pericosines are carbasugar‐type metabolites of Periconia byssoides OUPS‐N133, a fungus that was originally separated from the sea hare Aplysia kurodai . It has been reported that pericosines C and E are enantiomeric mixtures. The difference in specific rotation between natural pericosine C and the synthetic one led to the conclusion that natural pericosine C is an enantiomeric mixture. Meanwhile, the small specific rotation of natural pericosine B compared to that of the synthetic one led to the deduction that natural pericosine B might also be an enantiomeric mixture. Then, racemic pericosines B and C were synthesized, and the direct enantioseparation of these racemic carbasugars was conducted with CHIRALPAK® IA and CHIRALPAK® AY‐H, which are suitable columns for racemic pericosines B and C, respectively. Using chiral HPLC, we conclude that natural pericosines B and C exist as enantiomeric mixtures. A rare example of the application of direct chiral HPLC analysis to intact sugars or carbasugars was provided. Chirality 2011. © 2011 Wiley Periodicals, Inc." @default.
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- W2331261126 date "2011-01-01" @default.
- W2331261126 modified "2023-09-25" @default.
- W2331261126 title "Natural pericosines B and C as enantiomeric mixtures: Direct evidence by chiral HPLC analysis" @default.
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- W2331261126 doi "https://doi.org/10.1002/chir.20937" @default.
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