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- W2331664696 abstract "To better understand lattice disorder in hydrozincite, natural hydrozincite samples and synthetic analogues were investigated by XRD, FTIR, 13C MAS, and 13C CPMAS NMR. The size of coherent diffraction domains ranges between ~10 nm (Synth1) and ~30 nm (Synth2). FTIR peaks from the antisymmetric CO2-3 stretching v3 mode were observed at 1383 and 1515 cm-1 in all samples. Peaks due to OH vibrations were observed for all the samples at 3234, 3303, and 3363 cm-1, and were sharp only for the samples having larger crystal domains. The 13C MAS and CPMAS NMR spectra showed a main carbon signal at 164 ppm in the Synth2 sample, while two main signals were observed at ~164 and ~168 ppm in the Synth1 sample. The intensity ratio of the latter signals were found to be independent of contact time, in the investigated range between 0.2 and 30 ms." @default.
- W2331664696 created "2016-06-24" @default.
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- W2331664696 date "2013-07-01" @default.
- W2331664696 modified "2023-09-28" @default.
- W2331664696 title "Investigation of the hydrozincite structure by infrared and solid-state NMR spectroscopy" @default.
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- W2331664696 doi "https://doi.org/10.2138/am.2013.4158" @default.
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