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- W2331727838 abstract "空気中で高度難熱性を示すカルボラン複合含ケイ素高分子の熱架橋構造を推定する目的で, そのモデル分子であるポリ (フェニルビニルシリレンエチニレン-1,3-フェニレンエチニレン) の熱硬化構造を個体高分解能 1H, 13C, 29Si NMRおよび2次元1H-13Cシフト相関NMRを用いて調べた. その結果, このポリマーは2つの熱硬化反応, すなわち, (1) 主鎖のC≡C結合どうしのジエン反応によるナフタレン環の生成, (2) 主鎖のC≡C結合と側鎖のビニル基および側鎖のビニル基どうしの付加反応によるシクロヘキセンの生成, が同時に進行し, 高い熱安定構造を形成すると結論した. どちらの反応も, 150℃以下では進行せず, おもに250～450℃の熱処理温度で進行し, 450℃までには完全に終了する." @default.
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- W2331727838 title "Thermosetting Mechanism Study of Poly[(Phenylvinylsilylene)ethynylene-1,3-phenyleneethynylene] by Solid-State and High-Resolution 1H, 13C, 29Si NMR Spectroscopy." @default.
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