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• W2332548709 startingPage "8312" @default.
• W2332548709 abstract "The impact of pristine multiwalled carbon nanotubes (MWCNTs), an ionic liquid (IL), 1-butyl-3-methylimidazolium hexafluorophosphate [BMIM][PF6], and the ionic liquid-modified MWCNTs (IL-MWCNTs) on the crystallization behavior of melt-crystallized poly(vinylidene fluoride) (PVDF) has been investigated. Pristine MWCNTs accelerate crystallization of PVDF as an efficient nucleation agent, while the formed crystals are mainly nonpolar α crystal form with few polar β crystals. Incorporation of only ionic liquid results in depression of the PVDF melt crystallization rate due to the miscibility of IL with PVDF but leads to a higher content of polar crystals (β and γ forms) than MWCNTs. The ionic liquid and MWCNTs show significant synergetic effects on both the nucleation and the formation of polar crystals for PVDF by melt crystallization. Addition of IL-MWCNTs not only improves the MWCNTs dispersion in PVDF matrix but also increases the overall crystallization rate of PVDF drastically. More important, the melt-crystallized PVDF nanocomposites with IL-MWCNTs show 100% polar polymorphs but no α crystal forms. To the best of our knowledge, this is the first report on the achievements of full polar crystal form in the melt-crystallized PVDF without mechanical deformation or electric field. The IL to MWCNTs ratio and the IL-MWCNTs loading content effects on the crystallization behavior of PVDF in the nanocomposites were also studied. It is considered that the specific interactions between >CF2 with the planar cationic imidazolium ring wrapped on the MWCNTs surface lead to the full zigzag conformations of PVDF; thus, nucleation in polar crystals (β and γ forms) lattice is achieved and full polar crystals are obtained by subsequent crystal growth from the nuclei." @default.
• W2332548709 created "2016-06-24" @default.
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• W2332548709 date "2012-07-05" @default.
• W2332548709 modified "2023-10-18" @default.
• W2332548709 title "Impact of Ionic Liquid-Modified Multiwalled Carbon Nanotubes on the Crystallization Behavior of Poly(vinylidene fluoride)" @default.
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• W2332548709 doi "https://doi.org/10.1021/jp304166t" @default.
• W2332548709 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/22702652" @default.
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