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W2332574740 abstract "The stabilization of copper clusters in nanosized metal–organic framework crystals, Cu-Y(BTC), was achieved by a solvent-exchange approach, followed by hydrogen reduction. The formation of copper clusters in the Y(BTC) nanocrystals generated during the hydrogen reduction process was followed by UV–vis spectroscopy. The Cu-Y(BTC) nanocrystals were further assembled in thin films with a thickness of 250 nm. The distribution and size of the copper clusters in the films were studied by CO chemisorption, followed by FT-IR spectroscopy combined with transmission electron microscopy. It was shown that the copper clusters with a mean diameter of 6 nm were homogeneously distributed and stabilized in the Cu-Y(BTC) films. Further, the Cu-Y(BTC) films were utilized for detection of single harmful gases, such as CO, chloroform, and 2-ethylthiophene, or mixtures of two compounds. The high sensitivity, selectivity, and reversibility of the Cu-Y(BTC) films toward single CO, chloroform, and 2-ethylthiophene were demonstrated. Noteworthy, the Cu-Y(BTC) films exhibited a fast response toward CO, even in the presence of chloroform and 2-ethylthiophene, which was due to the high activity and accessibility of copper clusters. The response of Cu-Y(BTC) toward 2-ethylthiophene was slower in comparison with chloroform, which was attributed to the bigger size and higher viscosity of 2-ethylthiophene." @default.
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W2332574740 date "2012-07-25" @default.
W2332574740 modified "2023-09-24" @default.
W2332574740 title "Detection of Harmful Gases by Copper-Containing Metal–Organic Framework Films" @default.
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W2332574740 doi "https://doi.org/10.1021/jp3044016" @default.
W2332574740 hasPublicationYear "2012" @default.
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