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• W2332950666 endingPage "11747" @default.
• W2332950666 startingPage "11735" @default.
• W2332950666 abstract "Four different chiral diamino diethers synthesized from N-isopropyl valinol or N-isopropyl alaninol were lithiated with n-butyllithium in tetrahydrofuran or diethyl ether. Crystal structures of the dilithiated diamino diethers were determined by X-ray diffraction. Three dilithiated diamino diethers including (2S,2′S)-1,1′-(butane-1,4-diylbis(oxy))bis(N-isopropylpropan-2-amine) 7, (2S,2′S)-1,1′-(pentane-1,5-diylbis(oxy))bis(N-isopropylpropan-2-amine) 8, and (2S,2′S)-1,1′-(heptane-1,7-diylbis(oxy))bis(N-isopropyl-3-methylbutan-2-amine) 9 are dimers, whereas dilithiated (2S,2′S)-1,1′-(pentane-1,5-diylbis(oxy))bis(N-isopropyl-3-methylbutan-2-amine) 10 is a monomer. The lithium atoms in all crystal structures adopt a nonequivalent coordination protocol and exist in two different environments in which one of the lithium atoms is tetra-coordinated while the other one is tri-coordinated. The solution structures of the dilithiated diamino diethers are also characterized by a variety of NMR experiments including diffusion-ordered NMR spectroscopy (DOSY) with diffusion coefficient-formula (D-FW) weight correlation analyses and other one- and two-dimensional NMR techniques." @default.
• W2332950666 created "2016-06-24" @default.
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• W2332950666 date "2014-08-08" @default.
• W2332950666 modified "2023-09-26" @default.
• W2332950666 title "Chiral Lithium Diamides Derived from Linked N-Isopropyl Valinol or Alaninol" @default.
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• W2332950666 doi "https://doi.org/10.1021/ja505179y" @default.
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• W2332950666 hasPublicationYear "2014" @default.
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