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- W2333075478 abstract "2-t-Butoxy-3-thienyl carbinols have been prepared and their combined dealkylation and dehydration reactions studied. Treatment of the title compounds at 10° with dil HCl in dioxan-water solution produces 3-(1′-alkenyl)-2-t-butoxythiophenes. When the carbinols are heated to about 150° in the presence of p-toluenesulphonic acid, 3-(1′-alkenyl)-3-thiolene-2-ones and 3-alkylidene-4-thiolene-2-ones are formed. Mechanistic considerations for the dealkylation and dehydration reactions are given. A hetero-Diels-Alder reaction is presented which gives a new route to condensed heterocycles." @default.
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- W2333075478 date "1970-01-01" @default.
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- W2333075478 title "Thiophene chemistry—XVI" @default.
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- W2333075478 doi "https://doi.org/10.1016/s0040-4020(01)92876-5" @default.
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