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- W233320998 abstract "Abstract : Forty-eight compounds were synthesized and evaluated as potential antiradiation drugs. These compounds were mainly N-substituted derivatives of 2-aminoethanethiol and were supplied as the hydrochloride salts. The synthetic methods used were: (1) thiolethylation of amines and alkanolamines with ethylene sulfide; (2) amination of epoxides and alpha, omega-alkylene dihalides with 2-(Benzylthio)ethylamine, followed by debenzylation; and (3) alkylation of alkanolamines with benzyl 2-chloroethyl sulfide, followed by debenzylation. A study of the reaction variables in the ethylene sulfide thiolethylation of a simple aliphatic amine (n-hexylamine) was begun. The data indicate that high amine:episulfide molar ratios and long reflux periods favor formation of the monothiolethylated product in good yield. (Author)" @default.
- W233320998 created "2016-06-24" @default.
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- W233320998 date "1962-07-20" @default.
- W233320998 modified "2023-09-27" @default.
- W233320998 title "SYNTHESIS OF ANTIRADIATION DRUGS" @default.
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