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• W2333221569 abstract "AbstractTwo new complexes containing M(II) ammine cations (M = Ni, Cd) and octahedral rhenium(III) thiocyanoammine and thiocyanohydroxoammine cluster anions, [Ni(NH3)6][Re6S8(CN)4(NH3)2]∙2H2O (1) and [Cd(NH3)6][{Cd(NH3)5}{Re6S8(CN)4(OH)(NH3)}]2∙5H2O (2), have been synthesized by hydrothermal reactions starting from Cs1.83K2.17[Re6S8(CN)4(OH)2]∙2H2O. The compounds were structurally characterized by single-crystal X-ray diffraction analysis, elemental analysis, energy dispersive spectroscopy, and IR spectroscopy. Both compounds adopt monoclinic crystal structures composed from discrete ionic species which are held together by multiple hydrogen bonds between CN–, OH–, and NH3 ligands and lattice water. 2 consists of {Cd(NH3)5}2+ attached to the OH group of the [Re6S8(CN)4(OH)(NH3)]3– cluster anion via the Re–OH–Cd linkage.Keywords: Octahedral rhenium clusterNickelCadmiumAmmine complexCrystal structure FundingThis research was supported by the Russian Foundation for Basic Research [grant number 11-03-00157], and [grant number 11-03-91052]." @default.
• W2333221569 created "2016-06-24" @default.
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• W2333221569 date "2013-12-10" @default.
• W2333221569 modified "2023-09-26" @default.
• W2333221569 title "Ionic coordination complexes based on [Re₆S₈(CN)₄L₂]<i>^<i>n</i></i>^– (L = OH^–, NH₃; <i>n</i> = 2, 3) cluster anions, and Ni(II) and Cd(II) ammine cations" @default.
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• W2333221569 doi "https://doi.org/10.1080/00958972.2013.865025" @default.
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