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• W2334065874 abstract "27Al NMR is used to quantify coordination changes in CaAl2O4 glass pressure cycled to 16 GPa. The structure and coordination environments remain unchanged up to 8 GPa, at which 93% of the recovered glass exists as four-fold Al, whereas the remaining population exists as [5,6]Al. Upon densification, [5,6]Al comprises nearly 30% of observed Al, most likely through the generation of three-coordinated oxygen. Negligible changes are observed for the isotropic chemical shift ([4]Al ≈ 78.8 ppm, [5]Al ≈ 46.3 ppm, [6]Al ≈ 12.6 ppm) and average quadrupole coupling strengths with pressure. 3QMAS spectra suggest less distortion within the newly formed Al environments in comparison with [4]Al. The chemical shift of [4]Al suggests that the aluminate network remains fully polymerized in glasses quenched from pressures up to 16 GPa." @default.
• W2334065874 created "2016-06-24" @default.
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• W2334065874 date "2011-11-01" @default.
• W2334065874 modified "2023-09-25" @default.
• W2334065874 title "Characterizing Pressure-Induced Coordination Changes in CaAl₂O₄ Glass Using ²⁷Al NMR" @default.
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• W2334065874 doi "https://doi.org/10.1021/jp204840z" @default.
• W2334065874 hasPublicationYear "2011" @default.
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