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- W2334171950 abstract "Abstract A high yielding synthesis of 1,3-oxazinan-2-ones starting from 3-amino-1-propanols and ethylene carbonate (EC) in the presence of catalytic amount of triazabicyclodecene (TBD) is herein reported. The formation of six-membered cyclic carbonates was achieved by intermolecular cyclization reaction via double B Ac 2 mechanism. Cyclization reactions have been carried out in neat as EC acted both as solvent and reagent. Pure 1,3-oxazinan-2-ones were isolated in high yield by simple liquid-liquid extraction. Further purification can be achieved by recrystallization. The reaction resulted of general application on different substrates including an aryl bis(3-amino-proan-1-ol) compound." @default.
- W2334171950 created "2016-06-24" @default.
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- W2334171950 date "2016-03-01" @default.
- W2334171950 modified "2023-10-09" @default.
- W2334171950 title "1,3-Oxazinan-2-ones via carbonate chemistry: a facile, high yielding synthetic approach" @default.
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- W2334171950 doi "https://doi.org/10.1515/pac-2015-1004" @default.
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