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• W2334618319 abstract "The asymmetric total syntheses of the α-benzylidene-γ-butyrolactone natural products megacerotonic acid and shimobashiric acid A have been accomplished in nine and 11 steps, respectively, from simple, commercially available starting materials. The key step for each synthesis is the (arene)RuCl(monosulfonamide)-catalyzed dynamic kinetic resolution-asymmetric transfer hydrogenation (DKR-ATH) of racemic α,δ-diketo-β-aryl esters to establish the absolute stereochemistry. Intramolecular diastereoselective Dieckmann cyclization forms the lactone core, and ketone reduction/alcohol elimination installs the α-arylidene." @default.
• W2334618319 created "2016-06-24" @default.
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• W2334618319 date "2015-02-20" @default.
• W2334618319 modified "2023-09-23" @default.
• W2334618319 title "Asymmetric Total Syntheses of Megacerotonic Acid and Shimobashiric Acid A" @default.
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• W2334618319 doi "https://doi.org/10.1021/acs.orglett.5b00140" @default.
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