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• W2334647966 endingPage "3716" @default.
• W2334647966 startingPage "3711" @default.
• W2334647966 abstract "The data obtained by thermogravimetry (TG), differential thermal analysis (DTA), and X-ray diffraction (XRD) measurements of the stoichiometric mixture of LiNO3, NH4VO3, and NH4H2PO4 were analyzed by both the Flynn–Wall–Ozawa (FWO) and Friedman–Reich–Levi (FRL) methods. The whole solid state reaction process could be divided into four stages corresponding to α values of 0.03–0.20, 0.30–0.60, 0.70–0.80, and 0.90–0.99. The nucleation of LiVP2O7 (α = 0.70–0.80) is a determining step of the four-reaction processes, for which the mechanism of random nucleation and subsequent growth, described by the Avrami–Erofeev equation (n = 4) G(α) = [−ln(1 – α)]4, was assumed. Moreover, the Gibbs free energy of activation ΔG*, enthalpy of activation ΔH*, and entropy of activation ΔS* at maximum temperature of the peak for the determining step were 99.24 kJ·mol–1, 199.97 kJ·mol–1, and 136.30 J·mol–1·K–1, respectively. Finally, XRD analyses confirmed that the Li3V2(PO4)3 synthesized by the precursor route is a pure phase." @default.
• W2334647966 created "2016-06-24" @default.
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• W2334647966 date "2014-05-14" @default.
• W2334647966 modified "2023-10-17" @default.
• W2334647966 title "Kinetic Studies on the Synthesis of Monoclinic Li₃V₂(PO₄)₃ via Solid-State Reaction" @default.
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• W2334647966 doi "https://doi.org/10.1021/jp501516k" @default.
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• W2334647966 hasPublicationYear "2014" @default.
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