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• W2334821446 abstract "The copolymerization of carbon dioxide and indene oxide to yield poly(indene carbonate) has been achieved through the use of bifunctional cobalt(III) catalysts. When compared to our earlier studies utilizing the traditional binary (salen)Co(III)X/cocatalyst system, the bifunctional catalysts display large increases in activity and selectivity for polymer while maintaining good control (PDI < 1.2). The copolymerization reactions can proceed at 25 °C while maintaining >99% selectivity for poly(indene carbonate) production. Polymer samples have been achieved with Mns and Tgs of up to 9700 g/mol and 138 °C, respectively. This represents the highest Tg yet observed for polycarbonates produced from the coupling of CO2 and epoxides. Additionally, the activation energy for the direct coupling of indene oxide and CO2 to yield cis-indene carbonate employing the (salen)CrCl/n-Bu4NCl catalyst system was determined to be 114.4 ± 5.7 kJ/mol utilizing in situ ATR-FTIR." @default.
• W2334821446 created "2016-06-24" @default.
• W2334821446 creator A5041235330 @default.
• W2334821446 creator A5077255739 @default.
• W2334821446 date "2013-08-01" @default.
• W2334821446 modified "2023-10-12" @default.
• W2334821446 title "Synthesis of CO₂-Derived Poly(indene carbonate) from Indene Oxide Utilizing Bifunctional Cobalt(III) Catalysts" @default.
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• W2334821446 doi "https://doi.org/10.1021/ma4013779" @default.
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