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- W2334971177 abstract "A new and efficient synthesis of chloromethyl chlorosulfate (CMCS) from chloroiodomethane and chlorosulfonic acid is described. This process leverages a chlorosulfonic acid-mediated iodide oxidation to drive the equilibrating displacement process to full conversion. The resulting iodine byproduct is further oxidized and removed as iodate, to prevent iodide-induced decomposition of CMCS. This new process provides an efficient and scalable protocol for the preparation of CMCS in 92% solution yield and high purity (>99 GC area %)." @default.
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- W2334971177 date "2012-11-05" @default.
- W2334971177 modified "2023-09-27" @default.
- W2334971177 title "Development of a Process for the Preparation of Chloromethyl Chlorosulfate" @default.
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- W2334971177 doi "https://doi.org/10.1021/op300246d" @default.
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