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• W2335132514 endingPage "4473" @default.
• W2335132514 startingPage "4463" @default.
• W2335132514 abstract "The structural aspects of binding of anions such as halides (chloride, 1, and bromide, 2) and oxyanions (perchlorate, 3, and hydrogen sulfate, 4) with the protonated tris(amide) receptor L were carried out in detail. In all of these complexes, the hydrogen of protonated bridgehead nitrogen of the ligand is endo-oriented, forming a strong N–H···O hydrogen bond with an amide oxygen of a tripodal side arm, and binding of anions is primarily governed by N–H···anion and C–H···anion interactions involving multiple receptor cations. Furthermore, transformation of the charged complexes into a unimolecular capsule of L has also been accomplished in the presence of excess fluoride ion in dimethyl sulfoxide (DMSO) solution. Crystallographic analysis of fluoride complex [TBA(L·F)]2DMSO·4H2O (5; TBA = tetrabutylammonium) shows that F– is fully encapsulated within the tripodal cleft governed by six strong hydrogen bonds from the amide -NH and aryl -CH protons of the π-acidic receptor. 1H NMR titration experiments further provide evidence for the formation of the F– encapsulated receptor capsule from the charged complexes." @default.
• W2335132514 created "2016-06-24" @default.
• W2335132514 creator A5090210230 @default.
• W2335132514 creator A5091649468 @default.
• W2335132514 date "2011-09-02" @default.
• W2335132514 modified "2023-09-26" @default.
• W2335132514 title "Fluoride Selectivity Induced Transformation of Charged Anion Complexes into Unimolecular Capsule of a π-Acidic Triamide Receptor Stabilized by Strong N–H···F^– and C–H···F^– Hydrogen Bonds" @default.
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• W2335132514 doi "https://doi.org/10.1021/cg200679x" @default.
• W2335132514 hasPublicationYear "2011" @default.
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