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- W2335334080 abstract "The formation of a PdZn alloy from a 4.3% Pd/ZnO catalyst was characterized by combined in situ high-resolution X-ray diffraction (HRXRD) and X-ray absorption spectroscopy (XAS). Alloy formation started already at around 100 °C, likely at the surface, and reached the bulk with increasing temperature. The structure of the catalyst was close to the bulk value of a 1:1 PdZn alloy with a L1o structure (RPd−Pd = 2.9 A, RPd−Zn = 2.6 A, CNPd−Zn = 8, CNPd−Pd = 4) after reduction at 300 °C and above. The activity of the gas-phase hydrogenation of 1-pentyne decreased with the formation of the PdZn alloy. In contrast to Pd/SiO2, no full hydrogenation occurred over Pd/ZnO. Over time, only slight decomposition of the alloy occurred under reaction conditions." @default.
- W2335334080 created "2016-06-24" @default.
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- W2335334080 date "2011-04-12" @default.
- W2335334080 modified "2023-10-14" @default.
- W2335334080 title "Formation and Characterization of PdZn Alloy: A Very Selective Catalyst for Alkyne Semihydrogenation" @default.
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- W2335334080 doi "https://doi.org/10.1021/jp1103164" @default.
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