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- W2336596602 abstract "Thermally induced phase separation (TIPS) has been used to engineer the macrostructure of polysilane foams. Liquid-liquid phase separation during unidirectional solidification resulted in 10-60 {mu}m wide channels. Mesoporosity is also observed within the channel walls. Decreasing the polymer concentration resulted in incomplete formation of the channel walls. Several solvents were investigated yielding a variety of macrostructures. Faster cooling rates gave more narrow (10 {mu}m), less continuous channels. Due to the low melting point of the polysilanes a stabilization step was performed to prevent the foam from melting prior to decomposition during pyrolysis. Pyrolysis of these stabilized polysilane foams yields a porous ceramic. This porous ceramic contains the pore network originally induced into the polymer by the TIPS process." @default.
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- W2336596602 date "1996-10-01" @default.
- W2336596602 modified "2023-09-23" @default.
- W2336596602 title "Engineering macrostructure in ceramics" @default.
- W2336596602 hasPublicationYear "1996" @default.
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