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- W2337611794 abstract "2 Abstract: Lead titanate thin films have been deposited by spin coating on stainless steel substrate using the precursor sol, which was synthesized from acetylacetone chelating with titanium isopropoxide and ethylene glycol as a solvent, in the sol-gel process. The influence of film thickness, pyrolysis temperature, and heating rate on (the formation of thin films) microstructure and morphology of thin films have been systematically investigated. The phase purity, particle size, and morphology are studied using X-ray diffraction and scanning electron microscopy (SEM) measurements. It is observed that the preferred oriented thin films could be obtained by pyrolysis of wet films at 150°C and annealed at 600°C at a slow heating rate of 4°C/min. It is also confirmed from X-ray patterns that the tetragonal perovskite structure of the titanate exists without any impu- rity peaks in the films formed. The TGA/DSC curves of the PT precursor show weight loss of ~7% and two exotherms at 492 and 522°C. They are attributed to the crystallization of tetragonal PbTiO 3 . SEM shows that the PbTiO 3 thin films annealed at 600°C for 1 h crystallized well. The FTIR analysis showed the characteristic absorption bands of Pb-O groups at 663 cm −1 and Ti-oxo groups at 600 cm −1 ." @default.
- W2337611794 created "2016-06-24" @default.
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- W2337611794 date "2015-01-01" @default.
- W2337611794 modified "2023-09-27" @default.
- W2337611794 title "ORGANIC CHEMISTRY | RESEARCH ARTICLE Sol-gel synthesis and characterization of lead titanate films" @default.
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