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• W2337676564 startingPage "2714" @default.
• W2337676564 abstract "A stable dialkylphosphinyl radical, 2,2,5,5-tatrakis(trimethylsilyl)-1-phosphacyclopentan-1-yl (RH2P•), showed both irreversible one-electron oxidation and reduction peaks at −0.24 and −2.29 V vs ferrocene/ferrocenium couple. One-electron reduction of RH2P• with KC8 in the presence of 18-crown-6 (18-c-6) or [2.2.2]cryptand (crypt-222) gave the corresponding phosphides [K(18-c-6)]+[RH2P]− and [K(crypt-222)]+[RH2P]−. Whereas [K(18-c-6)]+[RH2P]− exists as a contact ion pair, [K(crypt-222)]+[RH2P]− exists as a solvent-separated ion pair in the solid state. Reaction of RH2P• with AgOTf afforded an unexpected product, a silver(I) phosphaalkene complex." @default.
• W2337676564 created "2016-06-24" @default.
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• W2337676564 date "2015-05-26" @default.
• W2337676564 modified "2023-10-18" @default.
• W2337676564 title "Redox Reactions of a Stable Dialkylphosphinyl Radical" @default.
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• W2337676564 doi "https://doi.org/10.1021/acs.organomet.5b00323" @default.
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