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• W2339478249 abstract "Ultramicroelectrode (UME) has a rapid response time to obtain electrochemical transient information. To obtain the real-time transient Raman information, we introduce the Au UMEs into the measurements of electrochemical surface-enhanced Raman spectroscopy (EC-SERS). However, the SEM and electrochemical results show that the roughened Au UMEs by conventional procedure for macroelectrodes will produce a microcavity because the enhanced mass transfer makes Au dissolved irreversibly. Thus, a roughening program based on pulse potential voltammetry is proposed to improve SERS activity of Au UMEs. We find a porous nanostructured film can be formed on the surface of Au UMEs, which exhibits good stability and stronger intensity in the EC-SERS experiments." @default.
• W2339478249 created "2016-06-24" @default.
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• W2339478249 date "2016-10-01" @default.
• W2339478249 modified "2023-10-14" @default.
• W2339478249 title "Electrochemically roughened gold microelectrode for surface-enhanced Raman spectroscopy" @default.
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• W2339478249 doi "https://doi.org/10.1016/j.jelechem.2016.04.008" @default.
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