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- W2340259322 abstract "Cs2PdSe8(1), a novel palladium polyselenide with a threedimensional open framework structure, has been synthesized via a solvothermal reaction using ethylenediamine as solvent. Its crystal structure has been determined by single crystal X-ray diffraction. The structure belongs to the tetragonal space group I41/acd (No. 142), a514.935(2), c512.907(3) As , V52897.0(8) As , Z58, R150.044, and wR250.063, for 640 unique reflections. The unique three-dimensional network is composed of two 3 =[Pd(Se4)2] 22 frameworks that are topologically identical and mutually insertional. Each framework is built upon by connecting the neighboring square-planar [Pd(Se4)2] units to generate an infinite assembly resembling alternating rightand lefthanded helices running along the c-axis. Thermal analysis (TGA) showed that compound 1 is stable up to 320 °C. Optical studies performed on the powder sample of 1 suggested that the compound is a semiconductor and a band gap of 1.5 eV was estimated from the diffuse reflectance data. ( 1998 Academic Press" @default.
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- W2340259322 date "1998-01-01" @default.
- W2340259322 modified "2023-09-26" @default.
- W2340259322 title "LETTER TO THE EDITOR Cs 2 PdSe 8 : A Unique Open Framework Structure with Double Helical Assemblies of (Pd(Se 4 ) 2 ) 22" @default.
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