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- W2340775953 abstract "The title complex, [Mn2 (Pie)4(DMF)8] (Pic=picrate anion), has been obtained by slow diffusion of diethyl ether into a DMF solution of the Mn(Pic)2A•6H2O and structurally characterized X-ray single-crystal diffraction. It crystallizes in the monoclinic, space group P2(1)/c with a=15.2561(12), b=19.6756(16), c=12.1328(10)A, β=94.4010(10)˚, V=3631.2(5) A^3, Z=2, C48H64Mn2N20O36, M(subscript r)=1607.07, D(subscript c)=1.470g/cm^3, F(000)=1660, μ=0.451mm^(-1), R=0.0424 and wR=0.1119 for 4595 observed reflections with I＞2σ(Ⅰ). There are two kinds of Mn(Ⅱ) ions which have the same coordination environment in the asymmetric unit cell. The Mn(Ⅱ) is coordinated by four carbonyl O atoms from the DMF molecules and two phenolate O atoms of the picrate anions, forming a distorted octahedral structure." @default.
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- W2340775953 date "2007-10-25" @default.
- W2340775953 modified "2023-09-27" @default.
- W2340775953 title "Crystal Structure of [Mn2 (Pic)4(DMF)8] Complex (Pic=picrate anion)" @default.
- W2340775953 hasPublicationYear "2007" @default.
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