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- W2341006076 abstract "A selective complexometric method is described for the determination of Tl(III) using sodium metabisulphite asreleasing agent. Thallium(III) and associated metal ions are complexed with excess EDTA and the surplus EDTA isback titrated at pH 5-6 (hexamine or acetic acid-acetate buffer) with standard zinc sulphate solution using xylenolorange as indicator. The addition of sodium metabisulphite displaces the EDTA selectively from the Tl-EDTA complex. The released EDTA, equivalent to Tl(III) present, is titrated with standard zinc sulphate solution. The results obtained are reproducible and accurate in the range 4-100 mg of thallium with relative error less than 0.30% and coefficient of variation not exceeding 0.40%. The proposed method is employed in the determination of thallium in its salts, complexes and synthetic mixture of metal ions." @default.
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- W2341006076 date "2006-02-01" @default.
- W2341006076 modified "2023-09-24" @default.
- W2341006076 title "COMPLEXOMETRIC DETERMINATION OF THALLIUM(III) USING SODIUM METABISULPHITE AS A SELECTIVE RELEASING AGENT" @default.
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