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- W2341357925 abstract "Ultra-fine mullite precursor powders were prepared by the hydrolysis of molecular-designed Al, Si-complex alkoxide. The surface areas of the resulting mullite powders derived from sol-gel route varied depending upon the aging and/or drying condition. This was due to the different agglomeration states of their primary particles, which precipitated by the hydrolysis of the precursor solutions. A thin electrical double layer was formed on the primary particles of the solvents with low dielectric constants, and then primary particles agglomerated into coarse secondary agglomerates, leading to mullite powders with high surface areas even after high-temperature calcination. A thick electrical double layer on the primary particles resulted in the uniform packing, which formed relatively dense secondary agglomerates during drying. This resulted in the lower surface areas when solvents with high dielectric constants were used during aging. This agglomeration behavior was confirmed by pore-size distributions and the observation of SEM of the mullite powders." @default.
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- W2341357925 date "1997-01-01" @default.
- W2341357925 modified "2023-10-02" @default.
- W2341357925 title "Preparation of Fine Mullite Powders with High Surface Area by Agglomeration Control of Alkoxide-derived Precursor Sol." @default.
- W2341357925 doi "https://doi.org/10.4164/sptj.34.170" @default.
- W2341357925 hasPublicationYear "1997" @default.
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