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• W2344609519 abstract "The average crystal structures of two natural porous titanosilicates of the labuntsovite group, lemmleinite-Ba and lemmleinite-K, ideally Na4K4Ba2Ti8(Si4O12)4O4(OH)4⋅8H2O and Na4K4K2Ti8(Si4O12)4O2(OH)6⋅8H2O, respectively, have been refined from single crystal X-ray diffraction data. Both samples represent an extensive solid solution with labuntsovite sensu strictu Na4K4D2Ti8(Si4O12)4O4(OH)4⋅10H2O where D = Mn, Fe, and Mg. In addition to the sharp Bragg reflections both crystals, space group C2/m, a = 14.3, b =13.8, c = 7.75 Å, β = 117°, exhibit diffuse layers at c*/2 intervals indicating faulty superstructures with c = 15.7 Å. The diffuse layers consist of two types of reflections. The dominant type is strongly diffuse and smeared along a* indicating an I-centered Bravais lattice. The other type is very sharp but also weak and is in agreement with a C-centered lattice. Models for both superstructures have been developed on the basis of crystal-chemical principles and their theoretical diffraction patterns have been calculated and compared with the observed diffuse layers yielding excellent qualitative agreement." @default.
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• W2344609519 date "2004-11-01" @default.
• W2344609519 modified "2023-09-25" @default.
• W2344609519 title "Origin of diffuse superstructure reflections in labuntsovite-group minerals" @default.
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• W2344609519 doi "https://doi.org/10.2138/am-2004-11-1210" @default.
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