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• W2345431354 endingPage "596" @default.
• W2345431354 startingPage "596" @default.
• W2345431354 abstract "A new general protocol for synthesis of fused 1,2,3-dithiazoles by the reaction of cyclic oximes with S₂Cl₂ and pyridine in acetonitrile has been developed. The target 1,2,3-dithiazoles fused with various carbocycles, such as indene, naphthalenone, cyclohexadienone, cyclopentadiene, and benzoannulene, were selectively obtained in low to high yields. In most cases, the hetero ring-closure was accompanied by chlorination of the carbocyclic moieties. With naphthalenone derivatives, a novel dithiazole rearrangement (15→13) featuring unexpected movement of the dithiazole ring from α- to β-position, with respect to keto group, was discovered. Molecular structure of 4-chloro-5H-naphtho[1,2-d][1,2,3]dithiazol-5-one 13 was confirmed by single-crystal X-ray diffraction. Electrochemical properties of 13 were studied by cyclic voltammetry and a complex behavior was observed, most likely including hydrodechlorination at a low potential." @default.
• W2345431354 created "2016-06-24" @default.
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• W2345431354 date "2016-05-06" @default.
• W2345431354 modified "2023-09-26" @default.
• W2345431354 title "Fused 1,2,3-Dithiazoles: Convenient Synthesis, Structural Characterization, and Electrochemical Properties" @default.
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• W2345431354 doi "https://doi.org/10.3390/molecules21050596" @default.
• W2345431354 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/6273032" @default.
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