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• W2346334150 abstract "A series of copper complexes ( 3 – 6 ) stabilized by 1,2,3-triazole-tethered N-heterocyclic carbene ligands have been prepared via simple reaction of imidazolium salts with copper powder in good yields. The structures of bi- and trinuclear copper complexes were fully characterized by NMR, elemental analysis (EA), and X-ray crystallography. In particular, [Cu 2 (L 2 ) 2 ](PF 6 ) 2 ( 3 ) and [Cu 2 (L 3 ) 2 ](PF 6 ) 2 ( 4 ) were dinuclear copper complexes. Complexes [Cu 3 (L 4 ) 2 ](PF 6 ) 3 ( 5 ) and [Cu 3 (L 5 ) 2 ](PF 6 ) 3 ( 6 ) consist of a triangular Cu 3 core. These structures vary depending on the imidazolium backbone and N substituents. The copper–NHC complexes tested are highly active for the Cu-catalyzed azide–alkyne cycloaddition (CuAAC) reaction in an air atmosphere at room temperature in a CH 3 CN solution. Complex 4 is the most efficient catalyst among these polynuclear complexes in an air atmosphere at room temperature." @default.
• W2346334150 created "2016-06-24" @default.
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• W2346334150 date "2016-05-03" @default.
• W2346334150 modified "2023-09-27" @default.
• W2346334150 title "Bi- and trinuclear copper(I) complexes of 1,2,3-triazole-tethered NHC ligands: synthesis, structure, and catalytic properties" @default.
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• W2346334150 doi "https://doi.org/10.3762/bjoc.12.85" @default.
• W2346334150 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/4901887" @default.
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