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- W2347818617 abstract "Objective To establish a high performance liquid chromatography method for simultaneous determination of anti-oxidants 1010,330,168,and 1076 in five-layer co-extrusion films used for infusion,and to study the migration of anti-oxidants to 0.9% sodium chloride injection.Methods The study was carried out by using RP-HPLC with Yilite C18 column(250 mm × 4.6 mm,5 μm) and acetonitrile-tetrahydrofuran-water(63:30:7) as mobile phase.The column temperature was 30 ℃,flow rate was 1 mL/min,detection wavelength was 276 nm,and injection volume was 10 μL.Results Under the chromatographic conditions used,anti-oxidants 1010,330,168,and 1076 had good linear relationship respectively in the following ranges of 0.6―253.6,0.6―246.4,0.6―257.6,and 0.6― 251.6 mg/L,and the average recoveries were 90.70%(RSD = 2.35%),89.11%(RSD = 2.75%),89.87%(RSD = 3.01%),and 92.78%(RSD = 1.81%).Conclusion This validated method is available for quality evaluation and quality control of anti-oxidants 1010,330,168,and 1076 in five-layer co-extrusion films used for infusion.The contents of four kinds of anti-oxidants in infusion films and raw materials meet the standards of European Pharmacopoeia.The migration contents of anti-oxidants to 0.9% sodium chloride injection are not detected." @default.
- W2347818617 created "2016-06-24" @default.
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- W2347818617 date "2012-01-01" @default.
- W2347818617 modified "2023-09-24" @default.
- W2347818617 title "Simultaneous determination and migration of four anti-oxidants in five-layer co-extrusion films used for infusion" @default.
- W2347818617 hasPublicationYear "2012" @default.
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