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- W2347821536 abstract "1,7-Cleve's acid was heated with the mixture of sodium hydroxide and potassium hydroxide at 250℃ for 5 hours in the atmosphere of nitrogen and in the presence of =0.6% additive TA as the tar and coke retarding agent to give 1-amino-7-naphthol with the purity of 96.3% and yield of 88.9%. The product was reacted with methyl chloroformate at 20-25℃ for 2 hours in the presence of tetrahydrofuran and sodium bicarbonate to give 1-methoxycarbonylamino-7-naphthol a dark grey powder of melting point 105-107℃,with the purity of 96.5% and yield of 76.4%." @default.
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- W2347821536 date "2005-01-01" @default.
- W2347821536 modified "2023-09-27" @default.
- W2347821536 title "A Process for Preparation of 1-Methoxycarbonylamino-7-naphthol" @default.
- W2347821536 hasPublicationYear "2005" @default.
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