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- W2348287105 abstract "Objective:To establish a quick,accurate,sensitive method for analysis of prednisone acetate,dexamethasone acetate,diclofenac sodium and ibuprofen mixed in antirheumatic traditional Chinese medicine by UPLC/MS/MS.Methods:The chromatographic conditions included ACQUITY BEH C18 analysis column(2.1 mm×50 mm,1.7 μm),mobile phase of 0.02 mol·L-1 ammonium acetate(A)and acetonitrile(B)with gradient elution,flow rate of 0.3 mL·min-1,the detection wavelength was set at 263 nm.Electrospay ionization(ESI)source was applied and operated in the positive and negative ion mode.Prednisone acetate,dexamethasone acetate,diclofenac sodium and ibuprofen mixed in traditional Chinese medicinal were identified.Results:Both prednisone acetate and diclofenac sodium were found in formulationgs.Conclusion:The method is sensitive and accurate,and can be used to detect the prednisone acetate,dexamethasone acetate,diclofenac sodium and ibuprofen mixed in antirheumatic traditional Chinese medicine." @default.
- W2348287105 created "2016-06-24" @default.
- W2348287105 creator A5069684954 @default.
- W2348287105 date "2010-01-01" @default.
- W2348287105 modified "2023-09-28" @default.
- W2348287105 title "UPLC/MS/MS determination of prednisone acetate,dexamethasone acetate,diclofenac sodium and ibuprofen mixed in antirheumatic traditional Chinese medicine" @default.
- W2348287105 hasPublicationYear "2010" @default.
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