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- W2348697726 abstract "To develop a method to measure trihexyphenidyl, chlorpromazine and clozapine in human blood with GC-MS.The specimens were alkalized (pH > 10) and extracted with V (benzene):V(ethyl acetate) = 1:1, and qualitatively analyzed using GC-MS-Full Scan with internal standard SKF525A. The specimens were alkalized (pH > 10) and extracted with V(benzene):V(ethyl acetate) = 1:1, and quantitatively analyzed using GC-MS-SIM with internal standard diazepam-d5.The lowest detection limits of trihexyphenidyl, chlorpromazine and clozapine were 0.3, 0.3 and 0.7 ng/mL (S/N > or = 3) respectively. The calibration curve in 20-10 000 ng/mL showed a good linear distribution. The recovery rate was 79.9% to 85.5%. The RSDs of intraday and interday were less than 5.1%.The established method was simple, sensitive and accurate for simultaneous determination of trihexyphenidyl, chlorpromazine and clozapine in human blood, and can be applied in forensic toxicological cases." @default.
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- W2348697726 date "2011-08-01" @default.
- W2348697726 modified "2023-09-27" @default.
- W2348697726 title "[Simultaneous determination of trihexyphenidyl, chlorpromazine and clozapine in blood by GC-MS]." @default.
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