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- W2349366980 abstract "A simultaneous method for the determination of 54 drugs residues(sulfonamides,nitroimidazoles,quinolones,macrolide antibiotics,lincosamides and praziquantel) in pork was developed and validated by high performance liquid chromatography-tandem mass spectrometry(HPLC-MS/MS) following solid phase extraction(SPE).The extracts were dissolved and distilled with acetonitrile.After that the supernatant solution was extracted with n-hexane to remove the fat,and then cleaned up with SPE C18 cartridges.The quantitative detection was performed on LC-MS/MS by multiple reaction monitoring(MRM) mode under positive electrospray ionization(ESI+).The one precursor/two product ion transitions were used for each compound.Isotopes dilution internal standard method was used to determine the residue contents in pork.The limits of quantification(LOQs) are 1.0 μg/kg(sulfonamides and nitroimidazoles),2.0 μg/kg(quinolones and lincosamides),3.0 μg/kg(macrolide antibiotics) and 0.3 μg/kg(praziquantel),respectively.Validation parameters are determined as follow correlation coefficients,which are more than 0.991,and the recovery for each analyte ranges of 20.9%—121% with relative standard deviations(RSDs) between 2.0% and 19.8%." @default.
- W2349366980 created "2016-06-24" @default.
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- W2349366980 date "2012-01-01" @default.
- W2349366980 modified "2023-09-23" @default.
- W2349366980 title "Simultaneous Determination of 54 Drugs Residues in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry and Isotopes Dilution Technique" @default.
- W2349366980 hasPublicationYear "2012" @default.
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