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- W2349731996 abstract "Cyclohexanone can react with 30% H2O2 to form adipic acid in the presence of Na2WO4·2H2O used as the catalyst.Sodium bisulfate was used as the acidic ligand in the reaction system for the first time.Main effects on the reaction such as the mole ratio of cyclohexanone and hydrogen peroxide,and the dosage of catalyst and sodium bisulfate,were investigated.It was found that the best mole ratio of cyclohexanone∶H2O2∶sodium tungstate∶sodium bisulfate was equal to 1∶4.94∶0.02∶0.02.The product yield could reach 82.2% after the reaction mixture was refluxed for 6 h.The yield was greater than many other ligands adopted in the same reaction system.Under the optimum reaction conditions the product yield was 83.6%,81.5% and 71.2%,respectively,upon using potassium bisulfate,sulfamic acid and p-toluene sulphonic acid as the ligands,which were advantageous in terms of low cost,low pollution,and reusability." @default.
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- W2349731996 date "2010-01-01" @default.
- W2349731996 modified "2023-09-27" @default.
- W2349731996 title "Application of sodium bisulfate in green synthesis of adipic acid" @default.
- W2349731996 hasPublicationYear "2010" @default.
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