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- W2349740970 abstract "Objective To establish a method for the determination of residual solvents in itraconazole transfersomes by gas chromatography(GC).Methods The detector was FID.The analytical column was DB-624(30 m ×0.32 mm,1.8 μm).The injector temperature was 200 ℃,and the detector temperature was set at 260 ℃.The column temperature was raised by temperature programming.Nitrogen served as carrier gas and the dimethylsulfoxide(DMSO) as solvent media.Results The two kinds of solvents had a good linearity in the experimental concentration.The detection limit of ethanol and chloroform was 1.58 and 2.968 μg·mL-1,respectively.The RSD of precision was less than 1.0% for both solvents.The average recovery was 98%-101%.Conclusion This method was simple,sensitive,accurate and can be used for the detection of residual solvents in itraconazole transfersomes." @default.
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- W2349740970 date "2013-01-01" @default.
- W2349740970 modified "2023-09-26" @default.
- W2349740970 title "Determination of Residual Solvents in Itraconazole Transfersomes by Gas Chromatography" @default.
- W2349740970 hasPublicationYear "2013" @default.
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