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- W2349747694 abstract "Objective:To establish a high performance liquid chromatographic method with charged aerosol detection(HPLC-CAD) for the determination of MSPC in vinorelbine liposome for injection,and to validate this method.Methods:A Waters e2695 Series HPLC system equipped with a charged aerosol detector was used.The samples were injected into a Venusil XBP-C8 column.The mobile phase was composed of methanol and distilled water with a flow rate of 1.0 mL·min- 1.The detector parameters included a gas pressure of 35 psi(house nitrogen)and a range of 200 pA.Results:The calibration curves were linear between 4.8 ~ 28.8 μg·mL- 1(r =0.9999).The repeatability and the intermediate precision RSD were less than 2.0%.The average recovery was 100.43%.Conclusion:This method is accurate,repeatable,convenient and rapid for the determination of 1-myristoyl-2-stearoylsn-glycero-3-phosphatidylcholine(MSPC) in vinorelbine liposome for injection.The charged aerosol detector is competent in the determination of lysolipid at low concentration." @default.
- W2349747694 created "2016-06-24" @default.
- W2349747694 creator A5052226445 @default.
- W2349747694 date "2014-01-01" @default.
- W2349747694 modified "2023-09-28" @default.
- W2349747694 title "Determination of lysolipid in vinorelbine liposome for injection by HPLC-charged aerosol detector" @default.
- W2349747694 hasPublicationYear "2014" @default.
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