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- W2349925111 abstract "LiFePO4 powder was synthesized by sol-gel and heating treatment process.The influences of sintering time on the microstructure,morphology and electrochemical performance were explored by XRD,SEM and galvanostatic charge-discharge.The results show that the stable sol and gel were prepared by PAA,FeNO3,LiNO3 and NH4H2PO4 in water solution.The LiFePO4 can be obtained under sintering at 650 ℃.With the increase of calcination time,LiFePO4 particle becomes larger and the crystal structure is more integrity.The LiFePO4 powder prepared by heating treatment gel at 650 ℃ for 16 h exhibits uniform distribution,high crystallinity,low agglomeration and high electrochemistry performance.The first discharge capacity reaches 140 mAh/g at the rate of 1C,and the capacity remains 130 mAh/g after 100 cycles.The capacity retention ratio reaches 93%,which can prove that LiFePO4 has stable cycle performance." @default.
- W2349925111 created "2016-06-24" @default.
- W2349925111 creator A5084237882 @default.
- W2349925111 date "2013-01-01" @default.
- W2349925111 modified "2023-09-23" @default.
- W2349925111 title "Preparation and Electrochemical Properties of LiFePO_4 Powder Prepared by Sol-gel Method" @default.
- W2349925111 hasPublicationYear "2013" @default.
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