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- W2350068077 abstract "Objective To develop a quantitative method for determination of pyrethroid insecticide(fenvalerate) and its metabolites(3-PBA) in human urine by high-performance liquid chromatography.Methods After acidification and C18 SEP-PAK solid phase extraction,the urine samples were analyzed by Zorbox SB C18 separation and DAD detector.Results A good liner relationship was obtained and the correlation coefficient were greater than 0.996.Relative standard deviation(RSD) and recoveries of fenvalerate and 3-PBA were both less than 10.0% and greater than 75%.Limit of detection of fenvalerate and 3-PBA were 0.78 μg/ml and 1.93 μg/ml respectively.Conclusion As it is convenient,low cost and reproducible,the method can meet biomonitoring requirements for general and special populations." @default.
- W2350068077 created "2016-06-24" @default.
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- W2350068077 date "2013-01-01" @default.
- W2350068077 modified "2023-09-24" @default.
- W2350068077 title "Determination of Pyrethroids and its Metabolites in Human Urine by High-Performance Liquid Chromatography" @default.
- W2350068077 hasPublicationYear "2013" @default.
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