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- W2350455057 abstract "Synthesis and crystal structure of title molecule is reported here. The crystal belongs to monoclinic, space group P 21/a with unit cell arameters of a = 0. 9771(2), b = 1. 6752(6), c = 1. 1552(3)nm,β= 109. 23(2)°, V= 1.785(2)nm3, Mr = 406. 21, Z = 4, Dx = 1. 42g/cm3. The final refinement converges with R = 0. 047 and Rω= 0. 051 for 1603 observed independent reflections. In this crystal, there is an intramolecular hydrogen bond between the amino and carbonyl group of N'H-C(S)-NH-C(O), which forms a planar six - membered ring and is parallel to the Cp ring of ferrocene moiety. The proton on N H(between phenyl and thiocarbonyl) gives δ 12.8 at lower field due to the intramolecular deshielding effect and that of NH ( between the carbonyl and thiocarbonyl)δ8.5 at high field." @default.
- W2350455057 created "2016-06-24" @default.
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- W2350455057 date "1996-01-01" @default.
- W2350455057 modified "2023-09-23" @default.
- W2350455057 title "Studies on Intramolecular Hydrogen Bond of N - Ferrocenoyl - N - 4 - acetyl phenyl thiourea" @default.
- W2350455057 hasPublicationYear "1996" @default.
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