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- W2350505239 abstract "o-Methoxycinnamic acid(OMA) was prepared by Claisen-Schmidt condensation of o-methoxybenzaldehyde(OMD)with acetone and then by Lieben haloform reaction of the intermediate o-methoxybenzalacetone(OMT)with NaClO.Acetone and OMD were condensed with a molar ratio of 2.5 at 20—30°C for 6hto obtain crude OMT,which was used directly in haloform reaction at 20—30°C for 8hto obtain OMA with a total yield of 81% after recrystallization fromφ=30% ethanol solution(GC purity 99.2%)." @default.
- W2350505239 created "2016-06-24" @default.
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- W2350505239 date "2014-01-01" @default.
- W2350505239 modified "2023-09-26" @default.
- W2350505239 title "Novel Two-Step Synthesis of o-Methoxycinnamic Acid" @default.
- W2350505239 hasPublicationYear "2014" @default.
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