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- W2350988054 abstract "New-style plasticizer tri(n-amyl) citrate was synthesized from citric acid and n-amyl alcohol using silica gel load-typed Ti(SO4)2,Zr(SO4)2,Fe2(SO4)3,Se(SO4)2 as the catalyst.Effects of esterification rate of different factors on the reaction were investigated.The results indicated that the amount of citric acid to n-amyl alcohol was 1 ∶ 4.0,the dosage of silica gel load Ti(SO4)2 was 3% of the total citric acid,the catalyst activation temperature was 400 ℃,the reaction temperature was 155~165 ℃,and the reaction time was 3.0 h,tri(n-amyl) citrate yield of 97.2% was attained,the purity determined by GC was over 99%.When the catalyst was repetitively used,the active didn't reduce obviously." @default.
- W2350988054 created "2016-06-24" @default.
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- W2350988054 date "2012-01-01" @default.
- W2350988054 modified "2023-09-28" @default.
- W2350988054 title "Synthesis of new-style plasticizer tri(n-amyl)citrate catalyzed by silica gel load-typed catalyst" @default.
- W2350988054 hasPublicationYear "2012" @default.
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