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- W2351106350 abstract "A ruthenium-diphosphine complex RuCl2(dppe)(NH2CH2CH2NH2)(1)(dppe=bis-(diphenyl-phosphino)ethane) was synthesized and characterized by 1H NMR and 31P NMR.As catalyst precursor,the catalytic performance of complex 1 was investigated for the hydrogenation of acetophnone in 2-propanol containing(CH3)3COK.The effect of various factors,such as reaction temperature(40-90 oC),hydrogen pressure(1-4 MPa) and molar ratio of(CH3)3COK to Catalyst(10∶1-200∶1) on the hydrogenation of acetophenone were studied.At the optimum conditions,S/C/(CH3)3COK=5000∶1∶40,70 oC,the conversion of acetophenone hydrogenation attained 99.6% in 5 h." @default.
- W2351106350 created "2016-06-24" @default.
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- W2351106350 date "2007-01-01" @default.
- W2351106350 modified "2023-09-23" @default.
- W2351106350 title "Preparation of ruthenium diphosphine complex RuCl_2(dppe)(NH_2CH_2CH_2NH_2) and its catalytic properties in hydrogenation of acetophenone" @default.
- W2351106350 hasPublicationYear "2007" @default.
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