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- W2351135918 abstract "Objective:To establish a method for determination of oleyl pyroglutamate and cyclo(Gly-Gln) in compound amino acids(15) and dipeptides(2) injection by HPLC.Methods:Aglient ZORBAX SB-C18(250 mm×4.6 mm,5 μm) column was adopted.The mobile phase was 0.01 mol·L-1 ammonium dibasic phosphate solution(adjust pH to 1.6 with phosphoric acid) at a flow rate of 1.0 mL·min-1,and the detection wavelength was 205 nm.Results:The method had a good linearity in the range of 25.15-503.0 mg·L-1 for oleyl pyroglutamate and 40.1-802.0 mg·L-1 for cyclo(Gly-Gln).The LODs(S/N=3) of oleyl pyroglutamate and cyclo(Gly-Gln) were 75.45 ng and 40.1 ng.The recoveries were 100.9% and 100.8%.Conclusion:The method is simple and accurate,and may be used to fast analysis of content determination." @default.
- W2351135918 created "2016-06-24" @default.
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- W2351135918 date "2011-01-01" @default.
- W2351135918 modified "2023-09-26" @default.
- W2351135918 title "HPLC determination of 2 impurities in compound amino acids(15) and dipeptides(2) injection" @default.
- W2351135918 hasPublicationYear "2011" @default.
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