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- W2351313612 abstract "An isocratic high-performance liquid-chromatographic method is-described for the simultaneously determining carbamazepine and its biologically active metabolite, carbamazepine-10, 11-epoxide. Serum samples containing an internal standard (10-methoxycarba-mazepine) are extracted with dichlor-methane and 4 mol · L-1 sodium hydroxide. The organic extract are evaporated at ambient temperature under a stream of nitrogen. The residues are reconstituted in mobile phase and injected on to a re-versed-phase C18 Column (150×4. 6mm I. D). The mobile phase consists of ace-tontrile/methanol/water (50/210/260 by vol) . The UV detector is operated at 214nm. The elution times of all com-pounds are within 7 min.The least detectable concentrations of carbamazepine and carbamazepine-10, 11-epoxide are 0. 08mg · L-1 and 0.1mg · L-1, respectively. The average absolute recovery for carbamazepine is 96.0% and for carbamazepine-10,11-epoxide is 97.3%. Within-run CV is 3. 3%~5.7%. and between-run CV is 4.3%~9.0%. The standard curve is linear at least within 40mg · L-1 for carbamazepine and within 20mg · L-1 for carbamazepine-10, 11-epoxide." @default.
- W2351313612 created "2016-06-24" @default.
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- W2351313612 date "1992-01-01" @default.
- W2351313612 modified "2023-09-23" @default.
- W2351313612 title "Determining carbamazepine and its active metabolite in human serum by HPLC method" @default.
- W2351313612 hasPublicationYear "1992" @default.
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