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- W2351599850 abstract "To establish a method for the determination of the concent ration of pyrogallol in serum by GC.The fixed liquid was 6% polydiethylene glycol succinate(DEGS),nitrogen as carrier gas,column initial temperature 170℃,after 3 minutes rising to 190℃ at the rate 20℃/ min,and holding for 3 minutes,then falling for 7 minutes.The injection chamber was 280℃,and the FID chamber was 280℃.The velocity of gas was: N2:40 mL/min,H2:70 mL/min,air:700 mL/min.The results showed that the calibration curve was linear in the concentration ranged from 16μg·mL-1 to 200μg·mL-1(r = 0.9967).The detection limit was 10μg·mL-1 and the method recoveries were from 80% to 98.71%.The RSD within a day was less than 3.31%and the RSD between days was less than 5.97%.The method is simple and precise,and can be used to detect the concentrations of pyrogallol in goats serum." @default.
- W2351599850 created "2016-06-24" @default.
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- W2351599850 date "2007-01-01" @default.
- W2351599850 modified "2023-09-25" @default.
- W2351599850 title "Determination of the Concentration of Pyrogallol in Serum by GC" @default.
- W2351599850 hasPublicationYear "2007" @default.
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