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- W2351736148 abstract "A measurement method for tetracyclines in sea perch involving LCMS/MS has been developed. The tetracyclines are extracted from sea perch using 1% perchloric acid and cleaned by solid-phase extractions prior to reversed-phase LC/MS/MS determination. Separation is performed on a Welch Materials Ultimate XB-C8 column using gradient elution with acetonitrile-methanol mixed solution and 0.1% formic acid. An agilent tandem mass spectrometer equipped with an electrospmy ionization source operated in multiple reaction monitoring(MRM) mode is utilized,and the results of determination are calculated from the calibration curve. The results of the LC/MS/MS method for the analysis of oxytetracycline,tetracycline,chlortetracycline,doxycycline in sea perch samples are as follows,the within-run RSD ranged from 0.12% to 0.86%,between-run RSD ranged from 0.10% to 0.37% and recoveries ranged between 91.7%~95.3%." @default.
- W2351736148 created "2016-06-24" @default.
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- W2351736148 date "2014-01-01" @default.
- W2351736148 modified "2023-09-26" @default.
- W2351736148 title "Determination of Oxytetracycline,Tetracycline,Chlortetracycline,Doxycycline in Sea Perch Aureomycin by LC/MS/MS" @default.
- W2351736148 hasPublicationYear "2014" @default.
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