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- W2351837360 abstract "A hyperbranched liquid polycarbosilane(HBPCS)with a low oxygen content was prepared by Grignard coupling of partially methoxylated chloromethyltrichlorosilane,followed by reduction with lithium aluminum hydride.The as-synthesized HBPCS was characterized by gel permeation chromatography(GPC),nuclear magnetic resonance(NMR)spectroscopy and elemental analysis.It is suggested that side reactions of THF and chlorosilanes can be avoided with the increase of methoxylation ratio.Less oxygen is expected in the precursors.Pyrolysis behavior of the HBPCS and crystallization behavior of the resultant ceramic were studied by means of thermal gravimetric analysis(TGA)and X-ray diffraction(XRD),respectively." @default.
- W2351837360 created "2016-06-24" @default.
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- W2351837360 date "2010-01-01" @default.
- W2351837360 modified "2023-09-26" @default.
- W2351837360 title "Synthesis and pyrolytic conversion of a hyperbranched liquid polycarbosilane with low oxygen content" @default.
- W2351837360 hasPublicationYear "2010" @default.
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