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- W2352003934 abstract "An optimized synthesis process of DMACA(N,N-dimethyla-cetamide dimethyl acetal) was reported.The process used liquid sodium methoxide,liquid sodium methoxide reacted with imine complex after steamed away methanol and then suspended in hexane.The molar ratio of sodium methoxide to dimethyl sulfate was 1.2 ∶1,the reaction temperature was-10 ℃,the dropping time was 1 h and the reaction time was 1.5 h.The yield was increased from 25%～35% to 75%～85%,and the purity of the product was over 98%." @default.
- W2352003934 created "2016-06-24" @default.
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- W2352003934 date "2011-01-01" @default.
- W2352003934 modified "2023-09-24" @default.
- W2352003934 title "Optimization for the synthesis of DMACA" @default.
- W2352003934 hasPublicationYear "2011" @default.
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